Special Topics: Advanced Forensic Chemistry
Fall 2005

03-498-4 Advanced Forensic Chemistry

Prerequisite: 03-225, 03-300 or 03-325

Lecture/Lab Hours: M: 6:30-9:00 PM 

Instructor: Dr. Salim M. Diab

Office: 815-740-3855 (St. Francis)

Home: 815-730-8302

Fax: 815-740-4285

Email: sdiab@stfrancis.edu

HomePage: http://www.stfrancis.edu/ns/diab/etherman.htm

Supplementary Lecture Notes:

www.stfrancis.edu/ns/diab/ForensicCoursePPT/lecturenotes.html
 

Course Description:

This is a special topics course in advanced forensic chemistry. The course will emphasize the theory, procedures, techniques, and applications of forensic chemistry, particularly as they relate to crime investigation and ongoing analysis of evidence obtained after a crime is committed. The nature of physical evidence is emphasized along with the limitations that technology and knowledge impose on its individualization and characterization. In order to merge theory with practice, a number of actual forensic case investigation will be analyzed.

 

Rationale and Objectives:

This course is designed to provide a basic scientific foundation in the field of forensic chemistry for those students in who are thinking of pursuing a criminal justice, forensic science, biology, or chemistry degree. Without having to major in chemistry, the student is allowed to experience the various analytical and instrumental methods used in investigating crimes.

 

Required Text:

Diab, S., Lab Manual: Advanced Forensic Chemistry:  Theory and Excercises. USF/Lewis University, 2005.
 

References:

Clifton E. Meloan, Richard E. James, and Richard Saferstein, "Criminalistics:An Introduction to Forensic Science", 7th Ed., Prentice-Hall, Inc., NY, 2001.
Baden, M. M.; Hennessee, J. A. Unnatural Death: Confessions of a Medical Examiner, Ballantine Books, New York, 1989.

Brewer, W. E.; Galipo, R. C.; Morgan, S. L.; Habben, K. H. "Confirmation of volatiles by solid-phase microextraction and GC/MS," J. Anal. Toxicol. 1997, 21(4), 286-290.

Davis, G. Forensic Science, American Chemical Society, Washington, DC, 1986.

Dwyer, J.; Kocieniewski, D.; Murphy, D; Tyre, P. Two Seconds Under the World: Terror Comes to America (The Conspiracy behind the World Trade Center Bombing, Crown Publishers, Inc., New York, 1994.

Evans, C. The Casebook of Forensic Detection, John Wiley & Sons, New York, 1996.

Fisher, D. Hard Evidence, Bantam DoubleDay Dell Publ. Group, NY, 1995.

Gerber, S. M., Ed., Chemistry and Crime; From Sherlock Holmes to Today's Courtroom, American Chemical Society, Washington, DC, 1984.

Ho, M. H. Analytical Methods in Forensic Chemistry, Ellis Horwood, Ltd., London, 1990.

Hunt, S. M. Investigation of Serological Evidence: A Manual for Field Investigators, Charles C. Thomas Publ. Ltd., London, 1984.

James, R. E. Laboratory Manual for Criminalistics, Prentice Hall, NY, 1980.

Lowry, W. T. Forensic Toxicology: Controlled Substances and Dangerous Drugs, Plenum Publ. Co., NY, 1979.

Maples, W. R.; Browning, M. Dead Men Do Tell Tales, Bantam DoubleDay, NY, 1994.

Saferstein, R. Forensic Science Handbook, Vol. I-III, Regents/Prentice Hall, NJ, 1993.

Tebbett, I., Ed., Gas Chromatography in Forensic Science, Ellis Horwood, Ltd., London, 1993.

Terry, I. M.; Robertson, J. C. Instrumental Data for Drug Analysis, CRC Press, Boca Raton, FL, 1991.

Wecht, C.; Curriden, M.; Wecht, B. Grave Secrets, Penguin books USA, Inc., New York, 1996.

Widmark, E. M. P. Principles and Applications of Medico-Legal Alcohol Determination, translated from original 1932 ed.,

Biomedical Publications, Davis, CA, 1981.

Yinon, J., Ed., Forensic Applications of Mass Spectrometry (Modern Mass Spectrometry), CRC Press, Boca Raton, FL, 1995.
 

WEB LINKS: http://www.stfrancis.edu/ns/diab/Forensic/sources.htm
 

Available Instruments/Equipment:

Refractometer

Digital Microscopes

Fingerprints Digital Sensor

UV light

UV-VIS Spectrophotometer

FT-IR Spectrophotometer/ ATR

GC-MS Spectrometer

TLC  Equipment

Electrophoretic Equipment

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Experiments/Exercises to be Performed:
 

                        1. Deductive Reasoning

                       

                        2. Glass and Soil Analysis

                       

                        3. Hair, Fiber, and Paint Analysis

 

                        4. Fingerprints Analysis

 

                        5. DNA Fingerprinting

                       

                        6. Spectroscopy: UV-VIS, IR, GC-MS

 

                        7. Toxicology and Drug Analysis

 

                        8. Arson: Analysis of Accelerants

Case Studies (Choose one case only):

                        9. Kidnapped: The Case of Jason Worth

 

                        10. The Case of Lois McArthur

 

                        11. Drug Bust

 

Assessment Questions:

 

                        Do all questions in back of Lab Manual

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Expectations of Students:

1. Attendance is required. A good attendance including the transcription of a good set of class notes will greatly improve the students' chances for achieving a satisfactory grade in this course.

2. Academic integrity must be always preserved. Any violation will be handled according to the guidelines in the College Catalog.

3. A complete and organized Lab. Report is due for all assigned labs.

4. Complete all assessment questions.

5. Review of Literature articles.

6. Final Exam - Presentations of class or research project:

 

References for research articles:

http://www.lib.jjay.cuny.edu/links/index.cfm?subid=167

http://ncstl.org

 

Breakdown for grading: 

                   Lab. Reports                     50%

                   Assessment Questions       30%

                   Presentations                     20%

                   Total                                 100%

Lab Pics: Summer 04:
Hair: 1, 2, 3, 4, 5, 6,7,8,9,10,11,12,13,14,15,16,17,18
Fiber: 1, 2, 3, 4, 5, 6, 7, 8, 9, 10, 11, 12, 13, 14, 15, 16, 17, 18, 19, 20

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